On the effects of fatigue precracking on the microstructure around precrack in 1TCT fracture toughness specimen of F82H-IEA

Tanigawa, Hiroyasu; Hashimoto, Naoyuki*; Sokolov, M. A.*; Klueh, R. L.*; Ando, Masami

Fusion Materials Semiannual Progress Report for the Period Ending (DOE/ER-0313/35), p.58 - 60, 2004/04

1TCT fracture toughness specimens of F82H-IEA steel were fatigue precracked and sliced in specimen thickness wise for microstructure analysis around the precrack. The microstructure around the precrack was observed by optical microscopy (OM), scanning electron microscopy (SEM), orientation imaging microscopy (OIM), and transmission electron microscopy (TEM). TEM samples around the crack front were prepared by focused ion beam (FIB) processor. The fracture surfaces of tested 1TCT specimens were also observed. OM observation showed that the precrack penetration was straight in the beginning, and then tended to follow a prior austenite grain boundary and to branch into 2 to 3 directions at the terminal. SEM and OIM observations revealed that the both microstructures around the precracks and ahead of the precrack had turned into cell structure, which is the typical microstructure of fatigue-loaded F82H. TEM images and inverse pole figures obtained from the crack-front region confirmed this structure change.